Hybrid Organometallic-Inorganic Nanomaterial: Acetyl Ferrocene Schiff base Immobilized on Silica Coated Magnetite Nanoparticles

Hybrid Organometallic-Inorganic Nanomaterial: Acetyl Ferrocene Schiff base Immobilized on Silica Coated Magnetite Nanoparticles

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In this work, a new hybrid organometallic-inorganic hybrid nanomaterial was prepared by immobilization of acetyl ferrocene on the surface of magnetite nanoparticles.Covalent grafting of silica coated magnetite nanoparticles (SCMNPs) with 3-aminopropyl triethoxysilane ORG SHIRITAKI SPAGHETTI W/OAT FIBRE gave aminopropyl-modified magnetite nanoparticles (AmpSCMNPs).Then, Schiff base condensation of AmpSCMNPs with acetyl ferrocene resulted in the preparation of acferro-SCMNPs hybrid nanomaterial.Characterization of the prepared nanomaterial was performed with different physicochemical methods such as Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), vibrating sample magnetometry (VSM), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), and transmission electron position-aids microscopy (TEM).

VSM analysis showed superparamagnetic properties of the prepared nanomaterial and TEM and SEM analyses indicated the relatively spherical nanoparticles with 15 nm average size.